N,N-二乙基-1,3-丙二胺合成路线 (共 7 条)
反应条件
potassium carbonate und Hydrieren des Reaktionsproduktes an Raney-Nickel;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2016
反应条件
in toluene T=110°C; 24 h;
参考文献
Osterloh, Frank; Saak, Wolfgang; Pohl, Siegfried
Journal of the American Chemical Society, 1997 , vol. 119, # 24 p. 5648 - 5656
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
1: aq. ethanol / 1 h / Heating 2: HCl / aq. ethanol / 10 h / Heating View Scheme
参考文献
Li, Chau-der; Mella, Sharon L.; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 9 p. 1089 - 1092
反应条件
1: With selenium T=20°C; P=750.075 Torr; 2 h; neat (no solvent); 2: With oxygen T=20°C; P=750.075 Torr; 1 h; neat (no solvent);
参考文献
Mizuno, Takumi; Nakai, Takeo; Mihara, Masatoshi
Synthesis, 2010 , # 24 art. no. F15510SS, p. 4251 - 4255
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US4918186 A1, 1990 ;
反应条件
in Petroleum ether stoich. amt., under nitrogene; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126