(2,2-二甲基丙基)苯合成路线 （共 75 条）
反应条件
aluminium trichloride; zinc in acetonitrile T=70°C; 20 h;
参考文献
Tetrahedron Letters, , vol. 43, # 24 p. 4391 - 4393
反应条件
aluminium trichloride; zinc in acetonitrile T=70°C; 20 h;
参考文献
Tetrahedron Letters, , vol. 43, # 24 p. 4391 - 4393
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate in benzene T=80°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 48, # 66 p. 8249 - 8251
反应条件
ZnCl2*(1,4-dioxane); 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride 1.) Et2O, 0 deg C, 15 min then room temp., 45 min, 2.) Et2O, reflux, 36 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 18 p. 4866 - 4870
反应条件
n-butyllithium; nickel; 2,4-xylyl tert-amyl sulfone 1.) THF, -78 deg C; 2.) THF, reflux, 8 h; 3.) 95percent ethanol, reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 108, # 12 p. 3466 - 3469
反应条件
ZnCl2*(1,4-dioxane); 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride 1.) Et2O, 0 deg C, 15 min then room temp., 45 min, 2.) Et2O, reflux, 36 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 18 p. 4866 - 4870
反应条件
n-butyllithium; 1-lt;(1,1-dimethylethyl)sulphonylgt;-2-methylbenzene; nickel 1.) THF, -78 deg C; 2.) THF, reflux, 8 h; 3.) 95percent ethanol, reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 108, # 12 p. 3466 - 3469
反应条件
n-butyllithium; nickel 1.) THF, -78 deg C; 2.) THF, reflux, 8 h; 3.) 95percent ethanol, reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 108, # 12 p. 3466 - 3469
反应条件
ZnCl2*(1,4-dioxane); 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride 1.) Et2O, 0 deg C, 15 min then room temp., 45 min, 2.) Et2O, reflux, 36 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 58, # 18 p. 4866 - 4870
反应条件
ZnCl2*(1,4-dioxane); 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride 1.) Et2O, 0 deg C, 15 min then room temp., 45 min, 2.) Et2O, reflux, 36 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 58, # 18 p. 4866 - 4870
