反应条件
1.1: H2O / 5 - 10 °C
1.2: 67 percent / acetic acid / H2O / 2 h / 20 °C
2.1: 39 percent / NH4Cl; NH4OH / acetonitrile / 3 h / Heating
3.1: 73 percent / S2Cl2 / dimethylformamide / 2 h / 80 °C
4.1: sodium hydrosulfide hydrate / dimethylformamide / 24 h / 100 °C
4.2: 72 percent / K2CO3 / dimethylformamide / 20 °C
View Scheme
参考文献
Jung, Myung Hee; Park, Jewn-Giew; Park, Woo-Kyu
Archiv der Pharmazie, 2003 , vol. 336, # 4-5 p. 230 - 235
