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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5-溴吲哚
合成路线
（共 206 条）
10075-50-0
5-溴吲哚
→
反应条件
66616-72-6
5-苯基-1H-吲哚
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran T=25°C; 1 h; Inert atmosphere;
参考文献
Manolikakes, Georg; Munoz Hernandez, Carmen; Schade, Matthias A.; Metzger, Albrecht; Knochel, Paul
Journal of Organic Chemistry, 2008 , vol. 73, # 21 p. 8422 - 8436
10075-50-0
5-溴吲哚
+
143-66-8
四苯硼钠
→
反应条件
66616-72-6
5-苯基-1H-吲哚
反应条件
palladium diacetate; sodium carbonate in various solvent(s) Suzuki reaction; 0.2 h; microwave irradiation;
参考文献
Villemin, Didier; Gomez-Escalonilla, Maria Jose; Saint-Clair, Jean-Francois
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 635 - 637
10075-50-0
5-溴吲哚
→
反应条件
81387-89-5
3,5-二溴吲哚
反应条件
bromine in N,N-dimethyl-formamide
参考文献
Hugon, Bernadette; Anizon, Fabrice; Bailly, Christian; Golsteyn, Roy M.; Pierre, Alain; Leonce, Stephane; Hickman, John; Pfeiffer, Bruno; Prudhomme, Michelle
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 17 p. 5965 - 5980
10075-50-0
5-溴吲哚
→
反应条件
81524-74-5
5-叠氮基吲哚
反应条件
sodium azide; CuSO4‵5H2O; sodium carbonate; sodium L-ascorbate; L-proline in water; N,N-dimethyl-formamide T=85°C;
参考文献
Liu, Yanghan; Xiao, Qicai; Liu, Yongqiang; Li, Zheng; Qiu, Yatao; Zhou, Guang-Biao; Yao, Zhu-Jun; Jiang, Sheng
European Journal of Medicinal Chemistry, 2014 , vol. 78, p. 248 - 258
10075-50-0
5-溴吲哚
→
反应条件
83515-06-4
5-溴-2-苯基-1H-吲哚
反应条件
(1,3-di(2,4,6-(CH3)3-C6H2)-imidazol-2-ylidene)Pd(OAc)2; acetic acid T=60°C; 15 h;
参考文献
Deprez, Nicholas R.; Kalyani, Dipannita; Krause, Andrew; Sanford, Melanie S.
Journal of the American Chemical Society, 2006 , vol. 128, # 15 p. 4972 - 4973
10075-50-0
5-溴吲哚
+
618-41-7
苯亚磺酸
→
反应条件
83515-06-4
5-溴-2-苯基-1H-吲哚
反应条件
sulfuric acid; silver(I) acetate; palladium dichloride in N,N-dimethyl-formamide; acetonitrile T=100°C; 0.666667 h; Sealed tubeMicrowave irradiation; regioselective reaction;
参考文献
Miao, Tao; Li, Pinhua; Wang, Guan-Wu; Wang, Lei
Chemistry - An Asian Journal, 2013 , vol. 8, # 12 p. 3185 - 3190
10075-50-0
5-溴吲哚
+
591-50-4
碘苯
→
反应条件
83515-06-4
5-溴-2-苯基-1H-吲哚
+
54470-19-8
反应条件
potassium acetate; palladium diacetate; bis(1,1-diphenylphosphino)methane in water T=110°C; 24 h; regioselective reaction;
参考文献
Joucla, Lionel; Batail, Nelly; Djakovitch, Laurent
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2929 - 2936
10075-50-0
5-溴吲哚
→
反应条件
851524-90-8
反应条件
1.1: trichlorophosphate / 0 - 35 °C 1.2: pH 10 / Cooling with ice 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Reflux 3.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C View Scheme
参考文献
BIOENERGENIX; MCCALL, John M.; ROMERO, Donna L.; KELLY, Robert C.
Patent: WO2012/119046 A2, 2012 ;
10075-50-0
5-溴吲哚
+
124-63-0
甲烷磺酰氯
→
反应条件
88131-63-9
反应条件
sodium hydride in N,N-dimethyl-formamide T=0 - 20°C;
参考文献
PALAU PHARMA, S. A.
Patent: WO2008/90181 A1, 2008 ;
Location in patent: Page/Page column 70 ;
WO 2008/090181 A1
10075-50-0
5-溴吲哚
+
98437-23-1
苯并噻吩-2-硼酸
→
反应条件
885273-14-3
5-(苯并噻吩-2-基)-1H-吲哚
反应条件
tri-tert-butyl phosphine; palladium diacetate; potassium hydroxide in tetrahydrofuran; water T=24°C; Suzuki-Miyaura Coupling; 0.0833333 h; Flow reactor;
参考文献
Nagaki, Aiichiro; Takabayashi, Naofumi; Moriwaki, Yuya; Yoshida, Jun-Ichi
Chemistry - A European Journal, 2012 , vol. 18, # 38 p. 11871 - 11875
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