1-(1,2,3,6-四氢-1-甲基-4-吡啶)-乙酮合成路线 （共 6 条）
反应条件
chromium(VI) oxide in acetic acid 1.25 h;
参考文献
Waters; Spivak; Hermsmeier; Yadav; Liang; Gund
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 545 - 554
反应条件
1: 81 percent / NaBH4 / methanol / 0.5 h / 21 °C 2: 18 percent / CrO3 / acetic acid / 1.25 h View Scheme
参考文献
Waters; Spivak; Hermsmeier; Yadav; Liang; Gund
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 545 - 554
反应条件
1: 90 percent / NaBH4 / ethanol / 1 h / 0 - 5 °C 2: 1percent aq. H2SO4 / 2 h / Ambient temperature View Scheme
参考文献
Beach, J. Warren
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1861 - 1863
反应条件
1: pyridine / CH2Cl2 / 2 h / Ambient temperature 2: tetrahydrofuran / 1.5 h / 0 °C View Scheme
参考文献
Ward; Merritt
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 6 p. 1709 - 1712
反应条件
in tetrahydrofuran T=0°C; 1.5 h; Yield given;
参考文献
Ward; Merritt
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 6 p. 1709 - 1712
反应条件
sulfuric acid 2 h; Ambient temperature;
参考文献
Beach, J. Warren
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1861 - 1863
