4-(羟基甲基)苄基氨基甲酸烯丙酯合成路线 （共 5 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 0.5 h; 2: With sodium hydroxide in tetrahydrofuran; water 0.25 h;
参考文献
LANTHEUS MEDICAL IMAGING, INC.; CESATI, Richard, R.; HARRIS, Thomas, D.; ROBINSON, Simon, P.; LOOBY, Richard, J.; CHEESMAN, Edward, H.; YALAMANCHILI, Padmaja; CASEBIER, David, S.
Patent: WO2011/5322 A2, 2011 ;
Location in patent: Page/Page column 63 ;
参考文献
Dogan, Zeynep; Paulini, Ralph; Stuetz, Jan A. Rojas; Narayanan, Sukunath; Richert, Clemens
Journal of the American Chemical Society, 2004 , vol. 126, # 15 p. 4762 - 4763
反应条件
1: 71 percent / LiAlH4 / tetrahydrofuran / 12 h / Heating 2: 67 percent / pyridine View Scheme
参考文献
Dogan, Zeynep; Paulini, Ralph; Stuetz, Jan A. Rojas; Narayanan, Sukunath; Richert, Clemens
Journal of the American Chemical Society, 2004 , vol. 126, # 15 p. 4762 - 4763
参考文献
Dogan, Zeynep; Paulini, Ralph; Stuetz, Jan A. Rojas; Narayanan, Sukunath; Richert, Clemens
Journal of the American Chemical Society, 2004 , vol. 126, # 15 p. 4762 - 4763
反应条件
1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C 2.2: 0.25 h View Scheme
参考文献
LANTHEUS MEDICAL IMAGING, INC.; CESATI, Richard, R.; HARRIS, Thomas, D.; ROBINSON, Simon, P.; LOOBY, Richard, J.; CHEESMAN, Edward, H.; YALAMANCHILI, Padmaja; CASEBIER, David, S.
Patent: WO2011/5322 A2, 2011 ;
