1-(3-甲氧苯基)-1-庚酮合成路线 （共 8 条）
反应条件
1: in tetrahydrofuran; diethyl ether; cyclohexane Heating / reflux; 2: With hydrogenchloride in tetrahydrofuran; diethyl ether; water T=0°C; Heating / reflux;
参考文献
Selwood, David; Visintin, Cristina; Baker, David; Pryce, Gareth; Okuyama, Masahiro
Patent: US2008/262011 A1, 2008 ;
Location in patent: Page/Page column 14 ;
US 20080262011 A1
反应条件
chromium(VI) oxide; sulfuric acid in water; acetone T=5 - 20°C; 3 h;
参考文献
Cheng, Li-Jie; Xie, Jian-Hua; Wang, Li-Xin; Zhou, Qi-Lin
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 6 p. 1105 - 1113
反应条件
in tetrahydrofuran; diethyl ether 6 h; Heating;
参考文献
Bourne, Caryl; Roy, Sucharita; Wiley, Jenny L.; Martin, Billy R.; Thomas, Brian F.; Mahadevan, Anu; Razdan, Raj K.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 24 p. 7850 - 7864
反应条件
1: magnesium / tetrahydrofuran / 3 h / 0 - 20 °C 2: chromium(VI) oxide; sulfuric acid / water; acetone / 3 h / 5 - 20 °C View Scheme
参考文献
Cheng, Li-Jie; Xie, Jian-Hua; Wang, Li-Xin; Zhou, Qi-Lin
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 6 p. 1105 - 1113
反应条件
1: magnesium / tetrahydrofuran / 3 h / 0 - 20 °C 2: chromium(VI) oxide; sulfuric acid / water; acetone / 3 h / 5 - 20 °C View Scheme
参考文献
Cheng, Li-Jie; Xie, Jian-Hua; Wang, Li-Xin; Zhou, Qi-Lin
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 6 p. 1105 - 1113
反应条件
chromium(VI) oxide; acetic acid
参考文献
Cardani et al.
Gazzetta Chimica Italiana, 1958 , vol. 88, p. 487,503
反应条件
diethyl ether Behandeln des Reaktionsgemisches mit wss.H2SO4;
参考文献
Fadia et al.
Journal of the Indian Chemical Society, 1955 , vol. 32, p. 117
参考文献
Cardani et al.
Gazzetta Chimica Italiana, 1958 , vol. 88, p. 487,503
