N-甲基-N-(吡啶-2-基)甲烷磺酰胺合成路线 (共 2 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C; 0.666667 h;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2004/11410 A1, 2004 ;
Location in patent: Page 126 ;
WO 2004/011410 A1
反应条件
N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in dichloromethane T=25°C; 15 h;
参考文献
Londregan, Allyn T.; Jennings, Sandra; Wei, Liuqing
Organic Letters, 2011 , vol. 13, # 7 p. 1840 - 1843