反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1732799', constants.ctx, '0')">carbon tetrabromide</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '610776', constants.ctx, '0')">triphenylphosphine</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0°C; 0.333333 h; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '1700556', constants.ctx, '0')">2-ethyl-capronaldehyde</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=23°C; 2 h; <br /> <br />
参考文献
MERCK PATENT GMBH; BLOUIN, Nicolas; MITCHELL, William; TOPLEY, Amy; TIERNEY, Steven Patent: WO2012/156022 A1, 2012 ; Location in patent: Page/Page column 69 ;