1-氮杂环十一烷-2-酮合成路线 （共 13 条）
反应条件
2,4,6-trichloro-1,3,5-triazine; zinc(II) chloride in acetonitrile Beckmann rearrangement; 1 h; Heating;
参考文献
Srivastava, Vishnu P.; Patel, Rajesh; Garima; Yadav, Lal Dhar S.
Chemical Communications, 2010 , vol. 46, # 31 p. 5808 - 5810
反应条件
sodium azide; sulfuric acid 2 h; Ambient temperature;
参考文献
Kalgutkar, Amit S.; Crews, Brenda C.; Marnett, Lawrence J.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1692 - 1703
反应条件
1: 80 percent / Et3N, DMAP / CH2Cl2 2: 68 percent / dimethylsulfoxide 3: 80 percent / LiAlH4 4: 92 percent / Et3N / CH2Cl2 5: 76 percent / nBu4NF / tetrahydrofuran 6: 75 percent / KMnO4 / DC-18-C-6 View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
反应条件
1: 68 percent / dimethylsulfoxide 2: 80 percent / LiAlH4 3: 92 percent / Et3N / CH2Cl2 4: 76 percent / nBu4NF / tetrahydrofuran 5: 75 percent / KMnO4 / DC-18-C-6 View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
反应条件
1: 92 percent / Et3N / CH2Cl2 2: 76 percent / nBu4NF / tetrahydrofuran 3: 75 percent / KMnO4 / DC-18-C-6 View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
反应条件
1: 80 percent / LiAlH4 2: 92 percent / Et3N / CH2Cl2 3: 76 percent / nBu4NF / tetrahydrofuran 4: 75 percent / KMnO4 / DC-18-C-6 View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
反应条件
1: 76 percent / nBu4NF / tetrahydrofuran 2: 75 percent / KMnO4 / DC-18-C-6 View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
反应条件
1: 75 percent / KMnO4 / DC-18-C-6 View Scheme
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
反应条件
Yield given. Multistep reaction;
参考文献
Huang; Wei, Huang; Kalivretenos; Kalivretenos, Aristotle G.
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9113 - 9116
反应条件
in tetrahydrofuran T=50°C; Title compound not separated from byproducts;
参考文献
Stehlicek, Jaroslav; Sebenda, Jan
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 9 p. 2524 - 2531
