[3-(吡啶-4-基)苯基]硼酸频那醇酯合成路线 （共 4 条）
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in 1,4-dioxane T=80°C; 24 h; Inert atmosphere;
参考文献
Su, Shi-Jian; Tanaka, Daisaku; Li, Yan-Jun; Sasabe, Hisahiro; Takeda, Takashi; Kido, Junji
Organic Letters, 2008 , vol. 10, # 5 p. 941 - 944
反应条件
1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 24 h / Reflux; Inert atmosphere 2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 24 h / 80 °C View Scheme
参考文献
INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTE
Patent: US2012/305901 A1, 2012 ;
反应条件
1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 24 h / Reflux; Inert atmosphere 2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 24 h / 80 °C View Scheme
参考文献
INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTE
Patent: US2012/305901 A1, 2012 ;
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; water; toluene Suzuki-Miyaura coupling; 24 h; Inert atmosphereReflux;
参考文献
Su, Shi-Jian; Tanaka, Daisaku; Li, Yan-Jun; Sasabe, Hisahiro; Takeda, Takashi; Kido, Junji
Organic Letters, 2008 , vol. 10, # 5 p. 941 - 944
