(2-甲氧基苯基)(哌嗪-1-基)甲酮合成路线 （共 5 条）
反应条件
trifluoroacetic acid
参考文献
VIFOR (INTERNATIONAL) AG
Patent: US2012/214798 A1, 2012 ;
反应条件
1: piperazine With n-butyllithium in tetrahydrofuran T=20°C; Metallation; 2: 2-methoxy-benzoyl chloride in tetrahydrofuran Acylation;
参考文献
Wang, Tao; Zhang, Zhongxing; Meanwell, Nicholas A.
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7661 - 7662
反应条件
1: triethylamine / diethyl ether 2: acetonitrile / 25 °C View Scheme
参考文献
Um, Ik-Hwan; Bae, Ae Ri
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7510 - 7515
反应条件
1: DIPEA; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate 2: trifluoroacetic acid View Scheme
参考文献
VIFOR (INTERNATIONAL) AG
Patent: US2012/214798 A1, 2012 ;
反应条件
in acetonitrile T=25°C; Kinetics;
参考文献
Um, Ik-Hwan; Bae, Ae Ri
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7510 - 7515
