反应条件
1: methyl 5-bromo-2-(methylthio)pyrimidine-4-carboxylate With 3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 1 h; 2: N-methylamine hydrochloride With N-ethyl-N,N-diisopropylamine in tetrahydrofuran; dichloromethane T=20°C;
参考文献
CHUA, Peter C.; Haddach, Mustapha; Nagasawa, Johnny Y.; Pierre, Fabrice; Whitten, Jeffrey P.
Patent: US2009/239859 A1, 2009 ;
Location in patent: Page/Page column 44 ;
US 20090239859 A1