反应条件
1: iodotrimethylsilane (TMSI) / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 2 h / 25 - 30 °C 2: 2.) MeOH / 1.) CH2Cl2, from 0 to 5 deg C, 3.5 h, 2.) from 0 to 5 deg C, 10 min View Scheme
参考文献
Walker, Donald G.; Brodfuehrer, Paul R.; Brundidge, Steven P.; Shih, Kun Mao; Sapino, Chester
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 983 - 991
