4 A molecular sieve; caesium carbonate; palladium dichloride in N,N-dimethyl-formamide T=100°C; Phenylation; 2 h;
参考文献
Satoh, Tetsuya; Inoh, Jun-Ichi; Kawamura, Yoshiki; Kawamura, Yuichiro; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 9 p. 2239 - 2246
4 A molecular sieve; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl-formamide T=130°C; Phenylation; 4 h;
参考文献
Satoh, Tetsuya; Inoh, Jun-Ichi; Kawamura, Yoshiki; Kawamura, Yuichiro; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 9 p. 2239 - 2246
1: With CpFe(CO)2(PCy3)*I; phenyl silane T=100°C; 24 h; IrradiationNeat (no solvent)Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran T=20°C; 1 h;
参考文献
Bezier, David; Venkanna, Gopaladasu T.; Castro, Luis C. Misal; Zheng, Jianxia; Roisnel, Thierry; Sortais, Jean-Baptiste; Darcel, Christophe
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 10 p. 1879 - 1884
