1,1-二甲氧基-2-苯基乙烷合成路线 (共 75 条)
反应条件
cation-exchange resin KU-2-8 T=20°C; 12 h;
参考文献
Yusubov; Zholobova; Filimonova; Chi, Ki-Whan
Russian Chemical Bulletin, 2004 , vol. 53, # 8 p. 1735 - 1742
反应条件
Decaborane in methanol T=20°C; 0.333333 h;
参考文献
Lee, Seung Hwan; Lee, Ji Hee; Yoon, Cheol Min
Tetrahedron Letters, 2002 , vol. 43, # 15 p. 2699 - 2703
反应条件
boron trifluoride diethyl etherate; IPy2BF4 in dichloromethane T=20°C; 0.0833333 h;
参考文献
Fananas, Francisco J.; Alvarez-Perez, Monica; Rodriguez, Felix
Chemistry - A European Journal, 2005 , vol. 11, # 20 p. 5938 - 5944
反应条件
hydroxylamine hydrochloride; sodium hydroxide T=20°C; 18 h; chemoselective reaction;
参考文献
Mickelsen, Ky J.; Tajc, Chelsea M.; Greenwood, Kevin R.; Browder, Cindy C.
Synthetic Communications, 2012 , vol. 42, # 2 p. 186 - 194
反应条件
pyridine; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; 16 h;
参考文献
Jin, Shiow-Jen; Arora, Pramod K.; Sayre, Lawrence M.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3011 - 3018
反应条件
3-chloro-benzenecarboperoxoic acid T=20 - 25°C; 1 h;
参考文献
Uemura, Sakae; Fukuzawa, Shin-ichi
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4347 - 4350
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Uemura, Sakae; Fukuzawa, Shin-ichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 471 - 480
反应条件
toluene-4-sulfonic acid in methanol 2 h; Heating;
参考文献
Mandai, Tadakatsu; Hara, Kiyomi; Nakajima, Tsukasa; Kawada, Mikio; Otera, Junzo
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 4993 - 4996
反应条件
toluene-4-sulfonic acid T=50 - 60°C; 0.5 h;
参考文献
Tarasova, O. A.; Mikhailova, A. I.; Shmidt, E. Yu.; Polovnikova, R. I.; Trofimov, B. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 6.1 p. 860 - 862
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 6 p. 807 - 809
反应条件
Me3SiOSO2F T=-78°C; 1.5 h;
参考文献
Lipshutz, Bruce H.; Burgess-Henry, Jana; Roth, Gregory P.
Tetrahedron Letters, 1993 , vol. 34, # 6 p. 995 - 998
反应条件
boron trifluoride diethyl etherate T=-5 - 20°C; 2 h;
参考文献
Burford, Clifford; Cooke, Frank; Roy, Glenn; Magnus, Philip
Tetrahedron, 1983 , vol. 39, # 6 p. 867 - 876