1,1-二甲氧基-2-苯基乙烷合成路线 (共 75 条)
反应条件
T=20°C; Irradiationactivation energie, ΔS(act.); Thermodynamic dataKineticsRate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1233 - 1240
参考文献
Justus Liebigs Annalen der Chemie, , vol. 560, p. 1,41
Journal of the Chemical Society, , p. 576,580
反应条件
T=50°C; 50 h; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 2 p. 163 - 170
反应条件
trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine in dichloromethane 0.05 h; Ambient temperature;
参考文献
Gassman, Paul G.; Burns, Stephen J.; Pfister, Keith B.
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1449 - 1457
参考文献
Sigmund; Uchann
Monatshefte fuer Chemie, 1929 , vol. 51, p. 245
反应条件
hydrogen; nickel T=180°C;
参考文献
Fleming,B.I.; Bolker,H.I.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 685 - 694
参考文献
Sigmund; Marchart
Monatshefte fuer Chemie, 1927 , vol. 48, p. 279
反应条件
1.1: t-BuOK; BuLi / hexane; tetrahydrofuran / 2 h / -95 °C 1.2: ClSnBu3 / hexane; tetrahydrofuran / 2 h / -95 - -50 °C 1.3: 0.13 g / LiCl; CuCl / Pd(PPh3)4 / dimethylsulfoxide / 2 h / 25 °C 2.1: 88 percent / Amberlyst-15 / CH2Cl2 / 1 h / 25 °C View Scheme
参考文献
Tivola, Paolo Balma; Deagostino, Anna; Prandi, Cristina; Venturello, Paolo
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 4 p. 437 - 441
反应条件
toluene-4-sulfonic acid T=60°C; Condensation; 12 h;
参考文献
Hinterberger, Sabine; Hofer, Otmar; Greger, Harald
Tetrahedron, 1998 , vol. 54, # 3-4 p. 487 - 496
反应条件
[rhenium(pentacarbonyl)(bromide)]; water in 1,2-dichloro-ethane T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Umeda, Rui; Nishi, Satoru; Kojima, Aya; Kaiba, Kenta; Nishiyama, Yutaka
Tetrahedron Letters, 2013 , vol. 54, # 2 p. 179 - 182