4-氨基-4'-硝基二苯基硫醚合成路线 （共 52 条）
反应条件
hydrogenchloride; potassium iodide; sodium nitrite
1.) 0 deg C, 1 h, 2.) 60 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Yuferov, A. M.; Akkuratova, O. L.; Sergeev, V. A.; Nedel'kin, V. I.; Yuferov, E. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2560 - 2562
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2794 - 2797
反应条件
1: tin; aqueous hydrochloric acid / Hydrogenation
2: acetic acid
3: potassium dichromate; aqueous sulfuric acid; acetic acid
View Scheme
参考文献
Sasosow; Galtschenko
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1946 , vol. 19, p. 580,583, 584
Chem.Abstr., 1947 , p. 2703
反应条件
1: dioxane; pyridine
2: aqueous hydrogen peroxide
View Scheme
参考文献
Schering Corp.
Patent: US2328548 , 1939 ;
反应条件
und Behandeln des Reaktionsprodukts mit wss. H2O2 in Essigsaeure;
参考文献
Farbenfabr.Bayer
Patent: DE895600 , 1941 ;
反应条件
dihydrogen peroxide; acetic acid
参考文献
Gabel'; Grinberg'
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1939 , vol. 12, p. 1481,1483
Chem.Abstr., 1940 , p. 6244
反应条件
1: 1.) aq. NaNO2, 7percent HCl, 2.) aq. KI / 1.) 0 deg C, 1 h, 2.) 60 deg C, 2 h
2: 2.) copper / 1.) methanol, reflux, 15 min, 2.) DMF, 140 deg C, 2 h
View Scheme
参考文献
Yuferov, A. M.; Akkuratova, O. L.; Sergeev, V. A.; Nedel'kin, V. I.; Yuferov, E. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2560 - 2562
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2794 - 2797
反应条件
2: aqueous H2O2
3: iron; aqueous acetic acid
View Scheme
参考文献
Farbenfabr. Bayer
Patent: DE895600 , 1941 ;
参考文献
Abbady, M. A.; Ali, M. M.; Kandeel, M. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 1 p. 53 - 57
反应条件
potassium carbonate in dichloromethane
T=5 - 6°C; 0.0833333 h;
参考文献
Kansy, M; Seydel, JK; Wiese, M; Haller, R
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 3 p. 237 - 244
反应条件
1: pyridine
2: und anschliessend mit wss. H2O2
3: Raney nickel / Hydrogenation
4: aqueous HCl
View Scheme
参考文献
Baker et al.
Journal of Organic Chemistry, 1950 , vol. 15, p. 400
