4-氨基-4’-甲氧基二苯胺合成路线 (共 26 条)
反应条件
titanium(III) chloride in 1,4-dioxane T=20°C; 4 h;
参考文献
Mizhiritskii, M. D.; Kuz'min, S. V.; Kogan, L. M.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 6.2 p. 1204 - 1205
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 6 p. 1340 - 1341
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos); ammonia; sodium t-butanolate in 1,4-dioxane T=110°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Lundgren, Rylan J.; Peters, Brendan D.; Alsabeh, Pamela G.; Stradiotto, Mark
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4071 - 4074
反应条件
gallium(III) chloride in dichloromethane T=20°C; 2 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 22 p. 5097 - 5104
反应条件
hydrogen fluoride; palladium
参考文献
Journal of the American Chemical Society, , vol. 77, p. 1762
US2714614 , ;
反应条件
sodium dithionite in tetrahydrofuran
参考文献
Benati, Luisa; Montevecchi, P. Carlo; Spagnolo, Piero
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1577 - 1582
反应条件
ammonium chloride; water; zinc
参考文献
Promysl.org.Chim., , vol. 2, p. 92,94
Chem. Zentralbl., , vol. 108, # I p. 850
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Chemische Berichte, , vol. 42, p. 1077
反应条件
1: 17 percent / di-t-butyl-hyponitrite / acetone / 48 h / 40 °C 2: 40 percent / 30percent aq. sodium dithionite / tetrahydrofuran View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1577 - 1582
反应条件
1: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux 2: stannous chloride-dihydrate; ethanol / 1 h / 70 °C / Inert atmosphere View Scheme
参考文献
Letters in Drug Design and Discovery, , vol. 9, # 4 p. 379 - 388
反应条件
1: sodium acetate / V methoxymethyl ester / 7 h / Inert atmosphere; Reflux 2: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux 3: stannous chloride-dihydrate; ethanol / 1 h / 70 °C / Inert atmosphere View Scheme
参考文献
Letters in Drug Design and Discovery, , vol. 9, # 4 p. 379 - 388