双(4-异氰酸酯基苯基)甲烷合成路线 (共 58 条)
反应条件
N-trimethyl-butyltetrafluoroboric acid; zinc oxide T=200 - 240°C; P=48.7549 Torr; 2.66667 h;
参考文献
LANZHOU INSTITUTE OF CHEMICAL PHYSICS, CHINESE ACADEMY OF SCIENCES
Patent: US2011/21810 A1, 2011 ;
Location in patent: Page/Page column 4 ;
反应条件
tetrabutylphosphonium bis(trifluoromethanesulfonyl)imide T=180 - 240°C; P=48.7549 Torr; 2.66667 h;
参考文献
LANZHOU INSTITUTE OF CHEMICAL PHYSICS, CHINESE ACADEMY OF SCIENCES
Patent: US2011/21810 A1, 2011 ;
Location in patent: Page/Page column 4 ;
反应条件
N,N-dimethyl-aniline; toluene
反应条件
2,4-bis(1,1-dimethylpropyl)phenol; dibutyl tin dilaurate T=220°C; P=9.75098 Torr; 15 h; Product distribution / selectivity;
参考文献
EP2088138 A1, ;
Page/Page column 53 ;
反应条件
in 1,2-dichloro-benzene T=185°C; P=760.051 Torr; 1.5 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2013/6013 A1, 2013 ;
Location in patent: Page/Page column 7 ;
反应条件
T=130 - 220°C; P=3.75038 - 450.045 Torr; 240 h; Product distribution / selectivity;
参考文献
Shinohata, Masaaki; Miyake, Nobuhisa
Patent: US2011/54211 A1, 2011 ;
Location in patent: Page/Page column 39 ;
反应条件
T=270°C; P=7.50075 Torr; Industry scale;
参考文献
EP2322504 A1, ;
Page/Page column 163; 172 ;
反应条件
T=260°C; P=11.2511 Torr; Industry scale;
参考文献
EP2322504 A1, ;
Page/Page column 127 ;
反应条件
T=260°C; P=11.2511 Torr; Industry scale;
参考文献
EP2322504 A1, ;
Page/Page column 129 ;
反应条件
T=240°C; P=6.0006 Torr; Industry scale;
参考文献
EP2322504 A1, ;
Page/Page column 132; 144 ;