4,4'-二甲氧基二苯安合成路线 (共 60 条)
反应条件
Cu2(OAc)2 in dichloromethane 2 h;
参考文献
Barton, Derek H. R.; Donnelly, Dervilla, M. X.; Finet, Jean-Pierre; Guiry, Patrick J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 9 p. 2095 - 2102
反应条件
CuI; potassium carbonate in dimethyl sulfoxide
反应条件
potassium tert-butylate; copper(l) iodide in toluene T=135°C; 14 h;
参考文献
Tetrahedron Letters, , vol. 43, # 40 p. 7143 - 7146
反应条件
in benzene-d6 T=95°C; 2 h; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 127, # 34 p. 12066 - 12073
反应条件
iron in acetic acid Heating;
参考文献
Alberti, Angelo; Greci, Lucedio; Stipa, Pierluigi; Sgarabotto, Paolo; Ugozzoli, Franco
Tetrahedron, 1987 , vol. 43, # 13 p. 3031 - 3040
反应条件
1: [bis(acetoxy)iodo]benzene / 0.08 h / 25 °C / |Schlenk technique; |Inert atmosphere 2: bismuth trifluoromethanesulphonate / methanol / 25 °C / |Schlenk technique; |Inert atmosphere 3: zinc; trifluoroacetic acid / methanol / 25 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 8 p. 2018 - 2021
反应条件
1: bismuth trifluoromethanesulphonate / methanol / 25 °C / |Schlenk technique; |Inert atmosphere 2: zinc; trifluoroacetic acid / methanol / 25 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 8 p. 2018 - 2021
反应条件
hydrogen fluoride; palladium Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 1762
反应条件
copper(l) iodide in pyridine 5 h; Heating;
参考文献
Journal of Physical Organic Chemistry, , vol. 7, p. 9 - 17
反应条件
alpha,alpha-dimethylbenzyl hydroperoxide Arrhenius parameters lg A3 and E3, enthalpie change ΔH3; Thermodynamic dataRate constantEquilibrium constant;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 4.1 p. 657 - 662
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 743 - 749