4,4'-二甲氧基二苯安合成路线 （共 60 条）
反应条件
tri-tert-butyl phosphine; sodium t-butanolate; palladium diacetate in xylene 4 h; Heating / reflux;
参考文献
Sony Corporation
Patent: US6337167 B1, 2002 ;
Location in patent: Example 8 ;
反应条件
[2,2']bipyridinyl; copper(l) iodide; potassium tert-butylate in toluene
参考文献
Newton, Graham N.; Mitsumoto, Kiyotaka; Wei, Rong-Jia; Iijima, Fumichika; Shiga, Takuya; Nishikawa, Hiroyuki; Oshio, Hiroki
Angewandte Chemie - International Edition, 2014 , vol. 53, # 11 p. 2941 - 2944
Angew. Chem., 2014 , vol. 53-126, # 11 p. 3093
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate in toluene T=130°C; 18 h; Inert atmosphere;
参考文献
Davies, Joshua A.; Elangovan, Arumugasamy; Sullivan, Philip A.; Olbricht, Benjamin C.; Bale, Denise H.; Ewy, Todd R.; Isborn, Christine M.; Eichinger, Bruce E.; Robinson, Bruce H.; Reid, Philip J.; Li, Xiaosong; Dalton, Larry R.
Journal of the American Chemical Society, 2008 , vol. 130, # 32 p. 10565 - 10575
反应条件
1: Pd2dba3; dppf; t-BuONa / toluene / 110 °C 2: 79 percent / POCl3 / 90 °C View Scheme
参考文献
Kauffman, Joel M.; Moyna, Guillermo
Journal of Organic Chemistry, 2003 , vol. 68, # 3 p. 839 - 853
反应条件
tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene 1 h; Ambient temperature;
参考文献
Hartwig, John F.; Kawatsura, Motoi; Hauck, Sheila I.; Shaughnessy, Kevin H.; Alcazar-Roman, Luis M.
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5575 - 5580
反应条件
Pd(dba)2 in ethyl acetate; toluene
参考文献
Yale University
Patent: US6100398 A1, 2000 ;
反应条件
iodine; copper; potassium carbonate Reagens 4: Nitrobenzol;
参考文献
Sasaki; Iyoda
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 272, p. 175 - 182
反应条件
pyridine; copper(l) iodide; n-butyllithium Yield given. Multistep reaction;
参考文献
Sasaki; Iyoda
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 272, p. 175 - 182
反应条件
tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate in toluene 3 h; Inert atmosphereReflux;
参考文献
Journal of Organic Chemistry, , vol. 77, # 4 p. 1663 - 1674
反应条件
iodine; sulfur in 1,2-dichloro-benzene T=150°C; 12 h;
参考文献
Yu, Lihai; Cui, Jinquan; Padakanti, Prashanth K.; Engel, Laura; Bagchi, Devika P.; Kotzbauer, Paul T.; Tu, Zhude
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 15 p. 4625 - 4634
