1,1’-亚甲基双(4-氯苯)合成路线 （共 54 条）
反应条件
sulfuric acid
T=40°C;
参考文献
Stephen; Short; Gladding
Journal of the Chemical Society, 1920 , vol. 117, p. 525
反应条件
silver tetrafluoroborate; tetraethyl tin in acetonitrile
168 h; Yield given. Yields of byproduct given;
参考文献
Reutov, O. A.; Uglova, E. V.; Mikhura, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 4 p. 825 - 828
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 4 p. 905 - 908
反应条件
boron trifluoride diethyl etherate
T=25°C; Friedel Crafts alkylation; 24 h; Inert atmosphere;
参考文献
Schaefer, Gabriel; Bode, Jeffrey W.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 46 p. 10913 - 10916
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in various solvent(s)
T=180°C; 3 h; Product distribution;
参考文献
Pri-Bar, Ilan; Buchman, Ouri; Schumann, Hebert; Kroth, Heinz J.; Blum, Jochanan
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4418 - 4428
反应条件
silver tetrafluoroborate in acetonitrile
168 h; Yield given. Yields of byproduct given;
参考文献
Reutov, O. A.; Uglova, E. V.; Mikhura, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 4 p. 825 - 828
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 4 p. 905 - 908
反应条件
0.0333333 h; microwave irradiation;
参考文献
Kundu, Sandip Kumar; Das, Suven; Pramanik, Animesh
Journal of Chemical Research, 2004 , # 11 p. 781 - 783
反应条件
silica gel supported phosphorus pentoxide
T=20°C; 0.166667 h; Neat (no solvent);
参考文献
Khazaei, Ardeshir; Rad, Mohammad Navid Soltani; Borazjani, Maryam Kiani; Moradian, Khadijeh Mansouri; Borazjani, Mohammad Kiani; Zebarjadian, Mohammad Hassan
South African Journal of Chemistry, 2011 , vol. 64, p. 120 - 126
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in various solvent(s)
T=180°C; 3 h; Product distributionRate constant;
参考文献
Pri-Bar, Ilan; Buchman, Ouri; Schumann, Hebert; Kroth, Heinz J.; Blum, Jochanan
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4418 - 4428
参考文献
Gaetzi; Stammbach
Helvetica Chimica Acta, 1946 , vol. 29, p. 563,570
反应条件
1: zinc chloride-monohydrate / 65 °C
2: concentrated sulfuric acid
View Scheme
参考文献
Stephen; Short; Gladding
Journal of the Chemical Society, 1920 , vol. 117, p. 525
