4,4'-二氨基二苯甲烷合成路线 （共 194 条）
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran; water T=20°C; 0.5 h;
参考文献
Organic Letters, , vol. 7, # 22 p. 5087 - 5090
反应条件
1: in water T=25 - 80°C; 2: With hydrogenchloride in water T=45 - 140°C; P=750.075 - 3750.38 Torr; 2.5 - 2.83333 h; 3: With sodium hydroxide in water T=100°C; Product distribution / selectivity;
参考文献
EP1734035 A1, ;
Page/Page column 5-6 ;
反应条件
1: With hydrogenchloride in water Heating / reflux; 2: With sodium hydroxide in water 0.25 h; Product distribution / selectivity;
参考文献
EP1707557 A1, ;
Page/Page column 5-9 ;
反应条件
1: With hydrogenchloride in water T=25 - 140°C; P=3750.38 Torr; 2.5 - 3.08333 h; 2: With sodium hydroxide in water T=100°C; Product distribution / selectivity;
参考文献
US2007/117997 A1, ;
Page/Page column 3; 4 ;
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Synthesis, , # 19 p. 3316 - 3340
反应条件
hydrogenchloride in water; cyclohexanone T=35 - 80°C;
参考文献
US2009/240077 A1, ;
Page/Page column 6 ;
反应条件
Iron (III) nitrate nonahydrate in methanol T=20°C; 24 h;
参考文献
European Journal of Organic Chemistry, , # 25 p. 4346 - 4351
反应条件
hydrogenchloride; water
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 775,779; engl.Ausg.S. 849,852
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 631,634; engl. Ausg. S. 641, 643
反应条件
hydrogenchloride; indium in tetrahydrofuran T=20°C; 24 h;
参考文献
Synthesis, , # 1 p. 81 - 84
反应条件
hydrogenchloride T=35 - 103°C; 11.0833 h; Heating / reflux;
参考文献
US2006/183938 A1, ;
Page/Page column 4 ;
