4,4'-二氨基二苯甲烷合成路线 (共 194 条)
反应条件
N,N-dimethyl-aniline; toluene
参考文献
BASF SE
Patent: US2009/281350 A1, 2009 ;
Location in patent: Page/Page column 3-4 ;
反应条件
1: H2SO4, (NH4)2SO4 2: toluene View Scheme
参考文献
Shinohata, Masaaki; Miyake, Nobuhisa
Patent: US2011/54211 A1, 2011 ;
反应条件
in chlorobenzene Heating;
参考文献
Bayer MaterialScience AG
Patent: US2009/240077 A1, 2009 ;
Location in patent: Page/Page column 6-7 ;
反应条件
in chlorobenzene 1.05556E-05 h;
参考文献
BASF SE
Patent: US2011/251425 A1, 2011 ;
Location in patent: Page/Page column 4 ;
参考文献
Eckert, Heiner; Forster, Barbara
Angewandte Chemie, 1987 , vol. 99, # 9 p. 922 - 923
反应条件
in chlorobenzene T=0°C; Product distribution / selectivity;
参考文献
EP1734035 A1, ;
Page/Page column 5-6 ;
反应条件
in chlorobenzene T=0°C; Heating / reflux; Product distribution / selectivity;
参考文献
Bayer MaterialScience AG
Patent: US2007/265465 A1, 2007 ;
Location in patent: Page/Page column 4-5 ;
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=25°C; 12 h; Inert atmosphere;
参考文献
Kimura, Tsutomu; Hosokawa-Muto, Junji; Kamatari, Yuji O.; Kuwata, Kazuo
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 5 p. 1502 - 1507
参考文献
Kaslow; Stayner
Journal of the American Chemical Society, 1946 , vol. 68, p. 2600
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Brode; Piper
Journal of the American Chemical Society, 1941 , vol. 3, p. 1502,1503
反应条件
T=150 - 155°C; 12 h;
参考文献
Mashraqui, Sabir H.; Nirantar, Swati S.; Biswas, Maloyesh M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 12 p. 1102 - 1104