4,4'-二氨基二苯甲烷合成路线 （共 194 条）
反应条件
hydrogen; 1 Ru/γ-Alumina T=110 - 130°C; P=104192 Torr; Product distribution / selectivity;
参考文献
WO2006/65961 A1, ;
Page/Page column 8-10 ;
反应条件
in chlorobenzene Heating;
参考文献
Bayer MaterialScience AG
Patent: US2009/240077 A1, 2009 ;
Location in patent: Page/Page column 6-7 ;
反应条件
in chlorobenzene T=0°C; Product distribution / selectivity;
参考文献
Bayer MaterialScience AG
Patent: EP1734035 A1, 2006 ;
Location in patent: Page/Page column 5-6 ;
反应条件
in chlorobenzene T=0°C; Heating / reflux; Product distribution / selectivity;
参考文献
Bayer MaterialScience AG
Patent: US2007/265465 A1, 2007 ;
Location in patent: Page/Page column 4-5 ;
反应条件
1: With sulfuric acid; potassium nitrate T=0°C; 3.5 h; 2: With ammonia in water T=0°C; Cooling with ice;
参考文献
Sudheesh Kumar
Oriental Journal of Chemistry, 2010 , vol. 26, # 4 p. 1393 - 1399
参考文献
Duval
Bulletin de la Societe Chimique de France, 1910 , vol. <4>7, p. 537
Full Text Show Details
Gram
Chemische Berichte, 1892 , vol. 25, p. 304
Full Text Show Details
Schnitzspahn
Journal fuer Praktische Chemie (Leipzig), 1902 , vol. <2>65, p. 316,317 Anm.3
反应条件
hydrogenchloride; sodium nitrite Eintragen der Reaktionsloesung in wss. Natriumsulfit-Loesung und Einleiten von Schwefeldioxid in das mit wss. Salzsaeure versetzte Reaktionsgemisch bei 70grad;
参考文献
Parkes; Morley
Journal of the Chemical Society, 1936 , p. 315
反应条件
N,N-dimethyl acetamide T=20 - 35°C; 3 h; Inert atmosphere;
参考文献
Kahvedzic, Amila; Nathwani, Seema-Maria; Zisterer, Daniela M.; Rozas, Isabel
Journal of Medicinal Chemistry, 2013 , vol. 56, # 2 p. 451 - 459
参考文献
Kaslow; Reck
Journal of the American Chemical Society, 1947 , vol. 69, p. 864
反应条件
hydrogenchloride in ethanol Acetylation;
参考文献
Schuetze, Dietrich; Sagelsdorff, Peter; Sepai, Ovnair; Sabbioni, Gabriele
Chemical Research in Toxicology, 1996 , vol. 9, # 7 p. 1103 - 1112
