Zhang, Jiadi; Bellomo, Ana; Creamer, Andrea D.; Dreher, Spencer D.; Walsh, Patrick J.
Journal of the American Chemical Society, 2012 , vol. 134, # 33 p. 13765 - 13772
potassium-sodium in ethylene glycol dimethyl ether
T=0°C; 3 h; Title compound not separated from byproducts;
参考文献
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853
potassium-sodium
1.) glyme, triglyme, 0 deg C, 3 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853
potassium-sodium
multistep reaction; analogous reaction with water quench (instead of (14)CH3I); possibility of sp2-sp3 carbon-carbon bonds cleavage; Product distribution;
参考文献
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853