1: N,N-dicyclohexylamine With n-butyllithium in tetrahydrofuran; hexanes
T=20°C; Inert atmosphere;
2: di-(2,6-di-isopropylphenyl)-carbodiimide in tetrahydrofuran; hexanes
RefluxInert atmosphere;
参考文献
Jin, Guoxia; Jones, Cameron; Junk, Peter C.; Lippert, Kai-Alexander; Rose, Richard P.; Stasch, Andreas
New Journal of Chemistry, 2009 , vol. 33, # 1 p. 64 - 75
Hickson, Clare L.; Keith, Eileen M.; Martin, Jane C.; McNab, Hamish; Monahan, Lilian C.; Walkinshaw, Malcolm D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1465 - 1470
1: 99 percent / acetonitrile / 5 h / Ambient temperature
2: 73 percent / 5 h / 600 °C / 0 - 0.01 Torr
View Scheme
参考文献
Hickson, Clare L.; Keith, Eileen M.; Martin, Jane C.; McNab, Hamish; Monahan, Lilian C.; Walkinshaw, Malcolm D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1465 - 1470