AlCl3, aluminium chloride in dichloromethane
T=0.5°C; Friedel Crafts acylation; 6 h; Cooling with iceReflux;
参考文献
Yu, Ming Ming; Li, Xia; Luan, Miao; Gao, Jun Na; Shi, Qiu Zhi; Tang, Ming Sheng; Wei, Liu He
Chinese Chemical Letters, 2010 , vol. 21, # 10 p. 1157 - 1161
1: diphenylether With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane
T=0 - 20°C; Inert atmosphere;
2: phenylphosphonous dichloride in diethyl ether; hexane
T=-78 - 20°C; Inert atmosphere;
参考文献
Dodds, Deborah L.; Boele, Maarten D.K.; Van Strijdonck, Gino P.F.; De Vries, Johannes G.; Van Leeuwen, Piet W.N.M.; Kamer, Paul C. J.
European Journal of Inorganic Chemistry, 2012 , # 10 p. 1660 - 1671
Toldov, S. V.; Kostenko, N. L.; Bel'skii, V. K.; Skvortsov, N. K.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 6 p. 1257 - 1265,1120 - 1127
Hitchcock et al.
Journal of the Chemical Society, 1957 , p. 4537,4544
Full Text Show Details
Oita; Gilman
Journal of the American Chemical Society, 1957 , vol. 79, p. 339,340
Kostenko, N. L.; Nesterova, S. V.; Toldov, S. V.; Skvortsov, N. K.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 3 p. 716 - 717,632 - 634
