3-苯基-1,3-噻唑烷-2,4-二酮合成路线 （共 72 条）
反应条件
in water
4 h; Heating;
参考文献
Singh, Harjit; Singh, Paramjit; Deep, Kanwal
Tetrahedron, 1983 , vol. 39, # 9 p. 1655 - 1660
反应条件
in water
7 h; Heating;
参考文献
Singh, Harjit; Singh, Paramjit; Deep, Kanwal
Tetrahedron, 1983 , vol. 39, # 9 p. 1655 - 1660
反应条件
hydrogenchloride
1 h; Heating;
参考文献
Matsubara, Yoshio; Nakamura, Toshiyuki; Yoshihara, Masakuni; Maeshima, Toshihisa
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 7 p. 3009 - 3011
反应条件
1: 77 percent / 1 h
2: 63 percent / sodium acetate / ethanol / 5 h / Heating
3: 23 percent / conc. aq. HCl / 1 h / Heating
View Scheme
参考文献
Turkevich, N. M.; Agaev, K. A.; Steblyuk, P. N.; Sementsiv, G. N.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 9 p. 668 - 670
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 9 p. 1068 - 1069
参考文献
Liebermann
Justus Liebigs Annalen der Chemie, 1881 , vol. 207, p. 140,141
反应条件
hydrogenchloride in 1,4-dioxane
1 h; Heating;
参考文献
Svetkin,Y.V. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1976 , vol. 12, p. 751 - 753
Khimiya Geterotsiklicheskikh Soedinenii, 1976 , vol. 12, p. 903 - 905
反应条件
1.1: Et3N / dimethylformamide / 10 h / 20 °C
1.2: 74 percent / ethanol / Heating
2.1: 55 percent / HCl / H2O / 0.5 h / 70 - 80 °C
View Scheme
参考文献
El'tsov; Mokrushin; Bel'skaya; Kozlova
Russian Chemical Bulletin, 2003 , vol. 52, # 2 p. 461 - 466
反应条件
1: 41 percent / sodium acetate / ethanol / Heating
2: 42 percent / HCl / H2O / 0.5 h / 70 - 80 °C
View Scheme
参考文献
El'tsov; Mokrushin; Bel'skaya; Kozlova
Russian Chemical Bulletin, 2003 , vol. 52, # 2 p. 461 - 466
反应条件
1: 99 percent / CH3COONa / ethanol / 2 h / Heating
2: conc. aq. HCl / ethanol / Heating
View Scheme
参考文献
Gursoy; Karali
Farmaco, 1995 , vol. 50, # 12 p. 857 - 866
反应条件
1: 63 percent / sodium acetate / ethanol / 5 h / Heating
2: 23 percent / conc. aq. HCl / 1 h / Heating
View Scheme
参考文献
Turkevich, N. M.; Agaev, K. A.; Steblyuk, P. N.; Sementsiv, G. N.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 9 p. 668 - 670
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 9 p. 1068 - 1069
