Schmeisser, M.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1947 , vol. 255, p. 33 - 44
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Gmelin Handbook: Cl: SVol.B2, 96, page 523 - 524
Bennett, G. M.; Brand, J. C. D.; Williams, G.
Journal of the Chemical Society, 1946 , p. 869 - 875
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Gmelin Handbook: S: MVol.B3, 71, page 1689 - 1691
in neat (no solvent) N2O5 (from P2O5 with HNO3); heating first to 50°C, at the end of reaction to 90°C;; drying on heating, removal of excessive iodine by sublimation; recrystallization in water several times, drying on heating to 220°C;;