sodium chloride in water; dimethyl sulfoxide T=180°C; 8 h;

1: 58 percent / NaCl / H2O; dimethylsulfoxide / 8 h / 180 °C 2: 54 percent / lithium aluminium monoethoxy hydride / diethyl ether 3: 60 percent / pyridine / 48 h View Scheme

1: 58 percent / NaCl / H2O; dimethylsulfoxide / 8 h / 180 °C 2: 54 percent / lithium aluminium monoethoxy hydride / diethyl ether View Scheme