1: sulfuryl dichloride / dichloromethane / 1 h / 0 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 1 h / 0 °C / Inert atmosphere View Scheme
参考文献
THE PENN STATE RESEARCH FOUNDATION; WANG, Hong-Gang; AMIN, Shantu; DOI, Kenichiro; GOWDA, Krishne; LOUGHRAN JR. , Thomas, P.
Patent: WO2013/112878 A1, 2013 ;
1: thionyl chloride; N,N-dimethyl-formamide / benzene / 2 h / Inert atmosphere; Reflux 2: AlCl3, aluminium chloride / dichloromethane / 0 - 25 °C / Inert atmosphere 3: sulfuryl dichloride / dichloromethane / 1 h / 0 °C / Inert atmosphere 4: boron tribromide / dichloromethane / 1 h / 0 °C / Inert atmosphere View Scheme
参考文献
THE PENN STATE RESEARCH FOUNDATION; WANG, Hong-Gang; AMIN, Shantu; DOI, Kenichiro; GOWDA, Krishne; LOUGHRAN JR. , Thomas, P.
Patent: WO2013/112878 A1, 2013 ;
1: AlCl3, aluminium chloride / dichloromethane / 0 - 25 °C / Inert atmosphere 2: sulfuryl dichloride / dichloromethane / 1 h / 0 °C / Inert atmosphere 3: boron tribromide / dichloromethane / 1 h / 0 °C / Inert atmosphere View Scheme
参考文献
THE PENN STATE RESEARCH FOUNDATION; WANG, Hong-Gang; AMIN, Shantu; DOI, Kenichiro; GOWDA, Krishne; LOUGHRAN JR. , Thomas, P.
Patent: WO2013/112878 A1, 2013 ;
1.1: pyridinium p-toluenesulfonate / 1,4-dioxane / 0.5 h / Reflux; Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere 2.2: 1 h / -78 °C / Inert atmosphere 3.1: AlCl3, aluminium chloride / dichloromethane / 0 - 25 °C / Inert atmosphere 4.1: sulfuryl dichloride / dichloromethane / 1 h / 0 °C / Inert atmosphere 5.1: boron tribromide / dichloromethane / 1 h / 0 °C / Inert atmosphere View Scheme
参考文献
THE PENN STATE RESEARCH FOUNDATION; WANG, Hong-Gang; AMIN, Shantu; DOI, Kenichiro; GOWDA, Krishne; LOUGHRAN JR. , Thomas, P.
Patent: WO2013/112878 A1, 2013 ;
