反应条件
1: sodium cyanoborohydride / acetic acid / 1 h / 20 °C / |Inert atmosphere
2: 4-(N,N-dimethlyamino)pyridine / acetic acid; dichloromethane / 5 h / 20 °C / |Inert atmosphere
3: boron trichloride / dichloromethane / 22 h / 0 - 20 °C / |Inert atmosphere
4: sodium dithionite; lithium hydroxide hydrate / water; tetrahydrofuran / 9 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Okano, Kentaro; Mitsuhashi, Nakako; Tokuyama, Hidetoshi
Tetrahedron, 2013 , vol. 69, # 51 p. 10946 - 10954