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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
101111-25-5
合成路线
（共 5 条）
101111-25-5
→
反应条件
28988-68-3
4-苄氧基-3-羟基苯乙酸
反应条件
water; copper; copper(II) oxide; potassium hydroxide T=140°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Sun, Haifeng; Zhu, Liyuan; Yang, Huicui; Qian, Wangke; Guo, Lin; Zhou, Shengbin; Gao, Bo; Li, Zeng; Zhou, Yu; Jiang, Hualiang; Chen, Kaixian; Zhen, Xuechu; Liu, Hong
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 4 p. 856 - 868
101111-25-5
→
反应条件
16562-14-4
3,9-二甲氧基-5,8,13,13alpha-四氢-6H-异喹啉并[3,2-a]异喹啉-2,10-二醇
反应条件
1.1: potassium hydroxide; water; copper; copper(II) oxide / 1 h / 140 °C / |Inert atmosphere; |Microwave irradiation 2.1: 3,4,5-trimethoxyphenylboronic acid / toluene / 1 h / |Reflux; |Dean-Stark 2.2: 46 h / 100 °C / |Molecular sieve; |Sealed tube 2.3: 2 h / |Reflux 3.1: potassium carbonate / acetone / 4 h / |Reflux 4.1: ethanol / 14 h / |Reflux 5.1: pyridine / dichloromethane / 1.5 h / 0 - 20 °C 6.1: trichlorophosphate / acetonitrile / 1 h / |Reflux; |Inert atmosphere 7.1: [[(η6-p-cymene)((1S,2S)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine)]Ru]; formic acid; triethylamine / N,N-dimethyl-formamide / 20 °C 8.1: water; sodium hydroxide / ethanol / 3 h / 20 °C 9.1: thionyl chloride / dichloromethane / 1.5 h / 0 - 20 °C 10.1: sodium hydrogencarbonate / dichloromethane / 1.5 h / 20 °C 11.1: hydrogenchloride / water; ethanol / 2 h / |Reflux View Scheme
参考文献
Sun, Haifeng; Zhu, Liyuan; Yang, Huicui; Qian, Wangke; Guo, Lin; Zhou, Shengbin; Gao, Bo; Li, Zeng; Zhou, Yu; Jiang, Hualiang; Chen, Kaixian; Zhen, Xuechu; Liu, Hong
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 4 p. 856 - 868
101111-25-5
→
反应条件
16562-14-4
3,9-二甲氧基-5,8,13,13alpha-四氢-6H-异喹啉并[3,2-a]异喹啉-2,10-二醇
反应条件
1.1: potassium hydroxide; water; copper; copper(II) oxide / 1 h / 140 °C / |Inert atmosphere; |Microwave irradiation 2.1: 3,4,5-trimethoxyphenylboronic acid / toluene / 1 h / |Reflux; |Dean-Stark 2.2: 46 h / 100 °C / |Molecular sieve; |Sealed tube 2.3: 2 h / |Reflux 3.1: potassium carbonate / acetone / 4 h / |Reflux 4.1: ethanol / 14 h / |Reflux 5.1: pyridine / dichloromethane / 1.5 h / 0 - 20 °C 6.1: trichlorophosphate / acetonitrile / 1 h / |Reflux; |Inert atmosphere 7.1: [[(η6-p-cymene)((1S,2S)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine)]Ru]; formic acid; triethylamine / N,N-dimethyl-formamide / 20 °C 8.1: water; sodium hydroxide / ethanol / 3 h / 20 °C 9.1: thionyl chloride / dichloromethane / 1.5 h / 0 - 20 °C 10.1: sodium hydrogencarbonate / dichloromethane / 1.5 h / 20 °C 11.1: hydrogenchloride / water; ethanol / 2 h / |Reflux View Scheme
参考文献
Sun, Haifeng; Zhu, Liyuan; Yang, Huicui; Qian, Wangke; Guo, Lin; Zhou, Shengbin; Gao, Bo; Li, Zeng; Zhou, Yu; Jiang, Hualiang; Chen, Kaixian; Zhen, Xuechu; Liu, Hong
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 4 p. 856 - 868
101111-25-5
→
反应条件
65615-22-7
反应条件
1.1: potassium hydroxide; water; copper; copper(II) oxide / 1 h / 140 °C / |Inert atmosphere; |Microwave irradiation 2.1: 3,4,5-trimethoxyphenylboronic acid / toluene / 1 h / |Reflux; |Dean-Stark 2.2: 46 h / 100 °C / |Molecular sieve; |Sealed tube 2.3: 2 h / |Reflux View Scheme
参考文献
SHANGHAI INSTITUTE OF MATERIA MEDICA, CHINESE ACADEMY OF SCIENCES; LIU, Hong; XIE, Xin; ZHEN, Xuechu; SUN, Haifeng; LI, Jing; ZHU, Liyuan; LI, Zeng; CHEN, Ying; JIANG, Hualiang; CHEN, Kaixian
Patent: US2014/88130 A1, 2014 ;
101111-25-5
→
反应条件
5884-48-0
反应条件
sodium hydroxide
参考文献
Hellmann,H.; Elser,W.
Justus Liebigs Annalen der Chemie, 1961 , vol. 639, p. 77 - 88
