2,2,2-三氯乙酸苯基酯合成路线 （共 11 条）
反应条件
triethylamine in tetrahydrofuran T=20°C;
参考文献
Imanishi, Takahiro; Fujiwara, Yuta; Sawama, Yoshinari; Monguchi, Yasunari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 771 - 776
参考文献
Shawali,A.S.A.S.; Biechler,S.S.
Journal of the American Chemical Society, 1967 , vol. 89, p. 3020 - 3026
反应条件
in tetrachloromethane 1.) 16 h, reflux, 2.) 48 h, 20 deg C;
参考文献
Blaschette, Armand; Linoh, Karin; Safari, Firouz; Schiebel, Hans-Martin
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1988 , vol. 43, # 12 p. 1639 - 1646
反应条件
hydrogenchloride T=20°C; 1 h; absence of HCl; MechanismProduct distribution;
参考文献
Gazizov, T. Kh.; Belyalov, R. U.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 8 p. 1673 - 1677,1355 - 1359
反应条件
hydrogenchloride T=100°C; 0.5 h; Mechanism;
参考文献
Gazizov, T. Kh.; Belyalov, R. U.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 8 p. 1673 - 1677,1355 - 1359
反应条件
T=50°C; 1 h; sealed ampule; Mechanism;
参考文献
Gazizov, T. Kh.; Belyalov, R. U.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 8 p. 1673 - 1677,1355 - 1359
参考文献
Houben
Chemische Berichte, 1926 , vol. 59, p. 2888
反应条件
palladium 10 on activated carbon; hydrogen in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 0.8 h; chemoselective reaction;
参考文献
Sawama, Yoshinari; Imanishi, Takahiro; Nakatani, Ryosuke; Fujiwara, Yuta; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2014 , vol. 70, # 30 p. 4540 - 4546
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Steglich,W. et al.
Chemische Berichte, 1967 , vol. 100, p. 1824 - 1832
反应条件
18-crown-6 ether; potassium carbonate T=90 - 150°C; 2 h;
参考文献
Renga, James M.; Wang, Pen-Chung
Synthetic Communications, 1984 , vol. 14, # 1 p. 77 - 82
