3-(4-氟苯基)-1-异丙基-1H-吲哚-2-苯甲醛合成路线 (共 8 条)
反应条件
sodium hydroxide; trichlorophosphate in hexane; water; N,N-dimethyl-formamide; toluene
反应条件
in dichloromethane; tert-butyl alcohol
参考文献
US5091378 A1, ;
US 5091378 A
反应条件
trichlorophosphate in 1,2-dichloro-ethane 16 h;
参考文献
Walkup, R. E.; Linder, J.
Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2155 - 2158
反应条件
tin(IV) chloride in dichloromethane 4.5 h; Heating;
参考文献
Walkup, R. E.; Linder, J.
Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2155 - 2158
反应条件
trichlorophosphate T=80°C; 18 h;
参考文献
Tetrahedron Letters, , vol. 26, # 18 p. 2155 - 2158
反应条件
1: 80.2 percent / dimethylformamide / 10 h / 100 °C 2: 81 percent / ZnCl2 / ethanol / 5 h / 100 - 105 °C 3: 52 percent / SnCl4 / CH2Cl2 / 4.5 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 18 p. 2155 - 2158
反应条件
1: 81 percent / ZnCl2 / ethanol / 5 h / 100 - 105 °C 2: 52 percent / SnCl4 / CH2Cl2 / 4.5 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 18 p. 2155 - 2158
反应条件
1: 80.2 percent / dimethylformamide / 10 h / 100 °C 2: 81 percent / ZnCl2 / ethanol / 5 h / 100 - 105 °C 3: 52 percent / SnCl4 / CH2Cl2 / 4.5 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 18 p. 2155 - 2158