N-(2,6-二氯苯基)甲酰胺合成路线 (共 4 条)
反应条件
acetic anhydride in dichloromethane 20 h; Ambient temperature;
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825
反应条件
in chloroform T=25°C;
参考文献
Vlietstra, Edward J.; Zwikker, Jan W.; Nolte, Roeland J. M.; Drenth, Wiendelt
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 12 p. 460 - 462
反应条件
thionyl chloride; sulfuryl dichloride T=60°C; 10 h; Inert atmosphere;
参考文献
Schann, Stephan; Greney, Hugues; Gasparik, Vincent; Dontenwill, Monique; Rascente, Carla; Lacroix, Gabriel; Monassier, Laurent; Bruban, Veronique; Feldman, Josiane; Ehrhardt, Jean-Daniel; Bousquet, Pascal
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 15 p. 4710 - 4715
反应条件
4-methyl-morpholine; trichloromethyl chloroformate in dichloromethane
T=-30°C; 1 h;
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825