N-2-(溴苯基)甲酰胺合成路线 （共 38 条）
反应条件
in toluene T=110°C; 4 h;
参考文献
STATE OF OREGON ACTING BY and THROUGH THE ST. BOARD OF HIGHER EDUCATION ON BEHALF OF THE UNIVERSITY OF OREGON; UNIVERSITY DISPLAY CORPORATION; LIU, Shih-Yuan; XU, Senmiao; KWONG, Raymond, C.
Patent: WO2014/4985 A1, 2014 ;
Location in patent: Page/Page column 57 ;
反应条件
choline chloride*2SnCl2 in water T=70°C;
参考文献
Azizi, Najmadin; Gholibeglo, Elham; Babapour, Mahbobe; Ghafuri, Hossein; Bolourtchian, Seyed Mohammad
Comptes Rendus Chimie, 2012 , vol. 15, # 9 p. 768 - 773
反应条件
sodium hydride in tetrahydrofuran T=20°C; 24 h;
参考文献
Lygin, Alexander V.; De Meijere, Armin
Organic Letters, 2009 , vol. 11, # 2 p. 389 - 392
反应条件
1: formic acid With acetic anhydride T=20 - 70°C; 3 h; 2: 1-Bromo-2-aminobenzene in tetrahydrofuran T=20°C; 1 h;
参考文献
WO2006/68058 A1, ;
Page/Page column 28-29 ;
反应条件
[bis(acetoxy)iodo]benzene in neat (no solvent) T=120°C; 0.333333 h; Microwave irradiationGreen chemistry;
参考文献
Vanjari, Rajeshwer; Kumar Allam, Bharat; Nand Singh, Krishna
RSC Advances, 2013 , vol. 3, # 6 p. 1691 - 1694
反应条件
palladium diacetate; triethylamine; di-(1-adamantyl)-n-butylphosphine in 1,4-dioxane T=120°C; P=7500.75 Torr; 16 h;
参考文献
He, Lin; Li, Haoquan; Neumann, Helfried; Beller, Matthias; Wu, Xiao-Feng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1420 - 1424
Angew. Chem., 2014 , vol. 126, # 5 p. 1444 - 1448,5
反应条件
pyridine T=100°C; Gleichgewicht und Geschwindigkeit der Reaktion;
参考文献
Zeitschrift fuer Physikalische Chemie, Stoechiometrie und Verwandtschaftslehre, , vol. 78, p. 362
Journal of the Chemical Society, , vol. 107, p. 733
反应条件
1: 1.) n-butyl-litjium / 1.) hexane, THF, -110 deg C; 2.) THF, hexane, 1 h, -105 deg C, 3 h, -78 deg C 2: 85 percent / 1.2M aq. potassium hydroxide / methanol / 1.5 h / Heating View Scheme
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Wallace, Ian H.M.; Michael, Joseph P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 349 - 360
反应条件
1: 45 percent / CuI, Et3N / Pd(PPh3)Cl2 / 5 h / 100 °C 2: 52 percent / NaOEt / ethanol / Heating View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Iwashita, Shigeki; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 5 p. 1823 - 1828
反应条件
diisopropylamine; trichlorophosphate in dichloromethane T=0°C; 0.25 h;
参考文献
Lygin, Alexander V.; De Meijere, Armin
Organic Letters, 2009 , vol. 11, # 2 p. 389 - 392
