(L)-2-二氮杂乙酰基吡咯烷-1-羧酸叔丁酯合成路线 （共 15 条）
参考文献
O'Neil, Ian A.; Murray, Clare L.; Potter, Andrew J.; Kalindjian, S. Barret
Tetrahedron Letters, 1997 , vol. 38, # 20 p. 3609 - 3610
反应条件
silver benzoate in 1,4-dioxane T=70°C; Wolff rearrangement; 6 h;
参考文献
Vasanthakumar, Ganga-Ramu; Patil, Basanagoud S.; Suresh Babu, Vommina V.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 18 p. 2087 - 2089
反应条件
silver benzoate; triethylamine T=-25 - 20°C; Rearrangement; Arndt-Eistert homologation; 3 h;
参考文献
Harrison, Justin R.; O'Brien, Peter; Porter, David W.; Smith, Neil M.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3623 - 3631
反应条件
silver benzoate; triethylamine
T=-25 - 20°C; Rearrangement; Arndt-Eistert homologation; 3 h;
参考文献
Harrison, Justin R.; O'Brien, Peter; Porter, David W.; Smith, Neil M.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3623 - 3631
反应条件
1: 99 percent / PhCOOAg; Et3N / 3 h / -25 - 20 °C
2: 16 percent / TFA / CH2Cl2 / 1.75 h / 0 - 20 °C
View Scheme
参考文献
Harrison, Justin R.; O'Brien, Peter; Porter, David W.; Smith, Neil M.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3623 - 3631
