1: 70 percent / POCl3 / 1,2-dichloro-ethane / 1 h / Heating 2: 2.) EtONa / 1.)165-170 deg C, 2 h 2.)r.t., 30 min View Scheme

palladium diacetate; triethylamine; biphenyl-2-yl-di-tert-butyl-phosphane in benzene T=100°C; 0.5 h; Inert atmosphere;

palladium diacetate; triethylamine; biphenyl-2-yl-di-tert-butyl-phosphane in benzene T=100°C; 0.116667 h; in sealed-cap vial; Reactivity;

<b>Multi-step reaction with 3 steps<br /> </b>1: K₂CO₃ / dimethylformamide / Ambient temperature<br />2: LiAlH₄ / tetrahydrofuran<br />3: SOCl₂ / CHCl₃ <br /> <br /> &nbsp;