1-(2-苯并噻唑基)-4-哌啶醇合成路线 (共 2 条)
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in ethylene glycol dimethyl ether T=70°C; 3 h;
参考文献
LG LIFE SCIENCES LTD.; KIM, Young Kwan; JOO, Hyun Woo; KIM, Myoung Yeol; PARK, Heui Sul; LEE, Tae Hee; KWAK, Hyo Shin; SHIM, Dong Sup; CHOI, Eun Sil
Patent: WO2012/111995 A1, 2012 ;
Location in patent: Page/Page column 30-31 ;
WO 2012/111995 A1
反应条件
1: dichloromethane / 2 h / 20 °C 2: caesium carbonate; 1,10-phenanthroline; copper(l) iodide / ethylene glycol dimethyl ether / 3 h / 70 °C View Scheme
参考文献
LG LIFE SCIENCES LTD.; KIM, Young Kwan; JOO, Hyun Woo; KIM, Myoung Yeol; PARK, Heui Sul; LEE, Tae Hee; KWAK, Hyo Shin; SHIM, Dong Sup; CHOI, Eun Sil
Patent: WO2012/111995 A1, 2012 ;
WO 2012/111995 A1