叔丁基-(2-碘乙氧基)二甲基硅烷合成路线 （共 10 条）
反应条件
1H-imidazole in dichloromethane T=20°C; 12 h;
参考文献
DRIVER, Michael; TARBIT, Brian; GEHRE, Alexander
Patent: US2013/59970 A1, 2013 ;
Location in patent: Paragraph 0311; 0312; 0313 ;
反应条件
sodium iodide in N-methyl-acetamide; acetone
参考文献
Driver, Michael; Hou, Qingpu; Wang, Jin Hai
Patent: US2013/59926 A1, 2013 ;
Location in patent: Page/Page column ;
反应条件
sodium iodide in acetonitrile T=-10 - 25°C; 24 h;
参考文献
Poleschner; Heydenreich; Martin
Synthesis, 1991 , # 12 p. 1231 - 1235
反应条件
1H-imidazole; iodine; triphenylphosphine in tetrahydrofuran T=0 - 20°C;
参考文献
Yamashita, Shuji; Iso, Kentaro; Kitajima, Kazuki; Himuro, Masafumi; Hirama, Masahiro
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2408 - 2425
反应条件
1H-imidazole in dichloromethane
参考文献
Desroches, Cedric; Lopes, Cesar; Kessler, Vadim; Parola, Stephane
Dalton Transactions, 2003 , # 10 p. 2085 - 2092
反应条件
1: imidazole / dimethylformamide / Ambient temperature 2: sodium iodide / acetone / 72 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1417 - 1424
反应条件
sodium iodide in acetone 72 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1417 - 1424
反应条件
n-butyllithium
1) hexane, THF, 2) HMPT, a) -30 deg C, 1 h, b) r.t., 3 h; Yield given. Multistep reaction;
参考文献
Poleschner; Heydenreich; Martin
Synthesis, 1991 , # 12 p. 1231 - 1235
