反应条件
1: glacial acetic acid, Br2 / methanol / 0 °C 2: acetic acid / 8 h / 60 - 65 °C 3: 45.6 percent / benzene / 2 h / Irradiation 4: sodium bicarbonate, manganous chloride, O2 / methanol; H2O / 0.75 h 5: 71.3 percent / 1) ceric ammonium nitrate / acetone / 2.5 h / 1) -10 degC, 2.5 h, 2) room temperature, ca. 45 min 6: benzene-d6 / 2 h / 5 °C / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 48, # 8 p. 1262 - 1266