11-氯-2,3-二氢-2-甲基-1H-二苯并[2,3:6,7]氧杂卓并[4,5-c]吡咯-1-酮合成路线 (共 2 条)
反应条件
AlCl3, aluminium chloride in chlorobenzene T=85°C; 9 h; SolventReagent/catalystTemperatureTime;
参考文献
WO2013/11461 A1, ;
Page/Page column 11-13 ;
反应条件
1: thionyl chloride / toluene 2: triethylamine / N,N-dimethyl-formamide 3: potassium tert-butylate / toluene 4: phosphoric acid; phosphorous pentoxide / toluene View Scheme
参考文献
Organic Process Research and Development, , vol. 12, # 2 p. 196 - 201