2,6-二(2-苯基乙烯基)吡啶合成路线 （共 8 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Heck reaction; 14 h;
参考文献
Chandrasekhar, Vadapalli; Narayanan, Ramakirushnan Suriya
Tetrahedron Letters, 2011 , vol. 52, # 27 p. 3527 - 3531
反应条件
acetic anhydride T=180°C; 41 h;
参考文献
Roblou, Emmanuel; Sasaki, Isabelle; Pezet, Frederic; Ait-Haddou, Hassan; Vincendeau, Sandrine
Synthetic Communications, 2004 , vol. 34, # 20 p. 3743 - 3749
反应条件
zinc(II) chloride T=225°C;
参考文献
Schuster
Chemische Berichte, 1892 , vol. 25, p. 2398
参考文献
Shaw
Journal of the Chemical Society, 1924 , vol. 125, p. 2363
Full Text Show Details
Ladenburg
Chemische Berichte, 1903 , vol. 36, p. 118
参考文献
Schuster
Chemische Berichte, 1892 , vol. 25, p. 2398
反应条件
1: With ozone in methanol; dichloromethane T=-70 - 20°C; 0.5 h; 2: 2,6-dibenzylidene-pyridine With tricyanoethylphosphine in methanol; dichloromethane T=20°C;
参考文献
Roblou, Emmanuel; Sasaki, Isabelle; Pezet, Frederic; Ait-Haddou, Hassan; Vincendeau, Sandrine
Synthetic Communications, 2004 , vol. 34, # 20 p. 3743 - 3749
反应条件
1.1: ozone / CH2Cl2; methanol / 0.5 h / -70 - 20 °C 1.2: 98 percent / tricyanoethylphosphine / CH2Cl2; methanol / 20 °C 2.1: methanol / 12 h / 20 °C 3.1: 90 percent / dimethyl sulfate; potassium carbonate / acetonitrile / 16 h / Heating View Scheme
参考文献
Roblou, Emmanuel; Sasaki, Isabelle; Pezet, Frederic; Ait-Haddou, Hassan; Vincendeau, Sandrine
Synthetic Communications, 2004 , vol. 34, # 20 p. 3743 - 3749
参考文献
Shaw
Journal of the Chemical Society, 1924 , vol. 125, p. 2363
Full Text Show Details
Schuster
Chemische Berichte, 1892 , vol. 25, p. 2398
