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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
101291-06-9
合成路线
（共 7 条）
14441-90-8
5-苯基-3-异恶唑羧酸
+
74497-02-2
→
反应条件
101291-06-9
反应条件
benzotriazol-1-ol; dicyclohexyl-carbodiimide in dichloromethane T=20°C; 24 h;
参考文献
Veeraswamy; Kurumurthy; Santhosh Kumar; Sambasiva Rao; Thelakkat, Kavya; Kotamraju, Srigiridhar; Narsaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 9 p. 1369 - 1375
→
反应条件
101291-06-9
反应条件
in 1,3,5-trimethyl-benzene T=160 - 170°C; 10 h; Heating;
参考文献
Shimizu, Tomio; Hayashi, Yoshiyuki; Ito, Takashi; Teramura, Kazuhiro
Synthesis, 1986 , # 6 p. 488 - 490
98-86-2
苯乙酮
→
反应条件
101291-06-9
反应条件
1: sodium methylate / methanol / 0 - 20 °C 2: hydroxylamine hydrochloride / methanol / 2 h / 50 °C 3: lithium hydroxide hydrate / tetrahydrofuran / 1 h / 50 °C 4: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 24 h / 20 °C View Scheme
参考文献
Veeraswamy; Kurumurthy; Santhosh Kumar; Sambasiva Rao; Thelakkat, Kavya; Kotamraju, Srigiridhar; Narsaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 9 p. 1369 - 1375
20577-73-5
2,4-二氧代-4-苯丁酸甲酯
→
反应条件
101291-06-9
反应条件
1: hydroxylamine hydrochloride / methanol / 2 h / 50 °C 2: lithium hydroxide hydrate / tetrahydrofuran / 1 h / 50 °C 3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 24 h / 20 °C View Scheme
参考文献
Veeraswamy; Kurumurthy; Santhosh Kumar; Sambasiva Rao; Thelakkat, Kavya; Kotamraju, Srigiridhar; Narsaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 9 p. 1369 - 1375
51677-09-9
5-苯基异噁唑-3-甲酸甲酯
→
反应条件
101291-06-9
反应条件
1: lithium hydroxide hydrate / tetrahydrofuran / 1 h / 50 °C 2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 24 h / 20 °C View Scheme
参考文献
Veeraswamy; Kurumurthy; Santhosh Kumar; Sambasiva Rao; Thelakkat, Kavya; Kotamraju, Srigiridhar; Narsaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 9 p. 1369 - 1375
3672-49-9
→
反应条件
101291-06-9
反应条件
sodium azide; chloroform; sulfuric acid
参考文献
Palazzo et al.
Annali di Chimica (Rome, Italy), 1959 , vol. 49, p. 853,855
101291-06-9
→
反应条件
14441-90-8
5-苯基-3-异恶唑羧酸
反应条件
potassium hydroxide
参考文献
Palazzo et al.
Annali di Chimica (Rome, Italy), 1959 , vol. 49, p. 853,855
