2-甲基-3-苯基喹喔啉合成路线 （共 31 条）
反应条件
1: 20 percent / NH3 / methanol / 40 - 50 °C
2: 69 percent / Na2S2O4 / methanol; H2O / 3 h / Heating
View Scheme
参考文献
Heyns, Kurt; Behse, Ernst; Francke, Wittko
Chemische Berichte, 1981 , vol. 114, # 1 p. 240 - 245
反应条件
1: 93 percent / 15-18percent NaOCl / 18 h
2: 20 percent / NH3 / methanol / 40 - 50 °C
3: 69 percent / Na2S2O4 / methanol; H2O / 3 h / Heating
View Scheme
参考文献
Heyns, Kurt; Behse, Ernst; Francke, Wittko
Chemische Berichte, 1981 , vol. 114, # 1 p. 240 - 245
反应条件
potassium tert-butylate in various solvent(s)
Ambient temperature;
参考文献
Consonni, Piero; Favara, Duccio; Omodei-Sale, Amedeo; Bartolini, Giuseppe; Ricci, Alfredo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 967 - 974
反应条件
sodium carbonate
T=20°C; 0.5 h;
参考文献
Lin, Pei-Ying; Hou, Rei-Sheu; Wang, Huey-Min; Kang, Iou-Jiun; Chen, Ling-Ching
Journal of the Chinese Chemical Society, 2009 , vol. 56, # 4 p. 683 - 687
参考文献
v. Auwers
Chemische Berichte, 1917 , vol. 50, p. 1180
反应条件
sodium acetate; acetic acid
参考文献
v. Auwers
Chemische Berichte, 1917 , vol. 50, p. 1180
反应条件
lithium
1) ether, RT, 90 min; 2) ether, RT, 1.30 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mettey, Yvette; Vierfond, Jean-Michel; Thal, Claude; Miocque, Marcel
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 133 - 137
参考文献
Boyer; Straw
Journal of the American Chemical Society, 1953 , vol. 75, p. 1642
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
Heating; Product distribution;
参考文献
Benati, Luisa; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Spagnolo, Piero; Strazzari, Samantha; Zanardi, Giuseppe; Calestani, Gianluca
Tetrahedron, 2002 , vol. 58, # 18 p. 3485 - 3492
反应条件
potassium tert-butylate in various solvent(s)
Ambient temperaturewithout reactant; Product distribution;
参考文献
Consonni, Piero; Favara, Duccio; Omodei-Sale, Amedeo; Bartolini, Giuseppe; Ricci, Alfredo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 967 - 974
