lithium tetramethylaluminate(III) in tetrahydrofuran T=25°C; 40 h;
参考文献
Matsubara, Seijiro; Nonaka, Tsuyoshi; Okuda, Yasuhiro; Kanemoto, Shigekazu; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1480 - 1483
lithium tetramethylaluminate(III) in tetrahydrofuran T=25°C; 40 h;
参考文献
Matsubara, Seijiro; Nonaka, Tsuyoshi; Okuda, Yasuhiro; Kanemoto, Shigekazu; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1480 - 1483
in tetrahydrofuran; diethyl ether; hexane soln. of stannane in THF added to soln. of (Me4Al)Li derived from Me3Al(1.0 M hexane soln.) and MeLi (1.5 M ether soln.) at 0°C, stirred for 40 h at 25°C, workup (1 M HCl, ether); SiO2 column chromy.;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 5 p. 1480 - 1483
in tetrahydrofuran; diethyl ether; hexane
soln. of stannane in THF added to soln. of (Me4Al)Li derived from Me3Al(1.0 M hexane soln.) and MeLi (1.5 M ether soln.) at 0°C, stirred for 40 h at 25°C, workup (1 M HCl, ether); SiO2 column chromy.;
参考文献
Matsubara, Seijiro; Nonaka, Tsuyoshi; Okuda, Yasuhiro; Kanemoto, Shigekazu; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1480 - 1483
