反应条件
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere 2: tetra-(n-butyl)ammonium iodide / pyridine / 0.5 h / 0 °C / Inert atmosphere 3: trifluoroacetic acid / dichloromethane / 0.13 h / 0 °C / Inert atmosphere 4: dichloromethane / 0.25 h / 20 °C / Inert atmosphere 5: dichloromethane / 19 h / 20 °C / Inert atmosphere 6: sodium methylate / methanol / 1.5 h / Reflux; Inert atmosphere View Scheme
参考文献
Darses, Benjamin; Greene, Andrew E.; Poisson, Jean-Francois
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 1710 - 1721